Moisture
measurement in lubricating oil is classically carried out in the laboratory
with a Karl Fischer titrator. Although Karl Fischer
titration is a primary standard, many challenges exist in making accurate and
timely measurements. Sampling technique and sampling frequency are critical
factors in determining the true condition of the oil. The accuracy of a Karl
Fischer titrator is not in question. The question is
whether the sample obtained for testing is representative. This poses a dilemma
for engineers wishing to obtain representative data in regard to the total
volume of oil that has passed through a lubrication system. Time between
samples, volume of sample, location of sample tap off and sample handling as well
as the repeatability of the method which relies 100% on company personnel
,raise doubts as to the validity of the practice – not the accuracy of
traceable laboratory analyzers. The Karl Fischer laboratory test is responsible
for measuring total water in an oil irrespective of
whether the sample that arrives at the laboratory is representative of the
total volume of oil that has passed through a filtration system. Serious
contenders in the oil and gas industry (although not related) took up the
challenge over 50 years ago with online water in oil monitors and automatic
sampling systems as opposed to total reliance on spot sampling methods. The
amount of of water for example in a crude oil can determine
the sales contract selling value of the product . Since millions of dollars are
being exchanged at any one time the complete reliance of a spot sample can be deemed invalid when
large amounts of loss or gained revenue are in question. This has spurred oil
companies to implement measurement teams with the sole responsibility to both
analyze online as well as in a laboratory.
The
need for a low cost device with virtually no maintenance, easily installed to
accurately measure total moisture /water content in oil has been the impetus in
the design and manufacture of EESIFLO’s new
generation water oil monitoring instruments. The EASZ-1 solution for industry
is continuous moisture measurement which eliminates questions raised by
sampling frequency and technique, since it is an instrument that electronically
samples the direct capacitance value of the water oil mixture every second and
correlates it to either a ppm
or percentage readout on a remote display or control system. The technology is
based on direct measurement of water in oil. Since water and oil have very
different dielectric strengths- the EASZ-1 measures the amount of energy that
can be stored in the liquid media which gives a true indication of moisture
level whether there is dissolved, emulsified or free water. Stability over
varying temperatures is resolved by temperature compensation.
Measuring
water in oil as a ppm value or percentage is a great
benefit to engineers. It enables them to correlate online information with Karl
Fischer test reports. Karl Fischer reports give information on total water
content irrespective of the form i.e. dissolved, emulsified or free.
Oil can hold a certain amount of moisture/water
but the ability of the oil to hold greater amounts of water over time increases
with oil aging. This increases the need to measure total water values which
correlate to Karl Fischer methods.
The
EASZ-1 is a temperature compensated online dielectric method of moisture analysis and is able
to measure the presence of water from 100ppm to 250,000 ppm
with a response time of 1 second . The sensing element consists of two
stainless steel barrels which act in a similar way to two separated plates
measuring dielectric. This enables a large volume of sample to be continuously
monitored as opposed to a small insert sensor which sees only a tiny fraction
of process media. Development of stable electronics to pick up minute changes
of water content in oil has been an activity of the company since the early
90’s. The result of much development and testing has produced a stable
measurement device that responds immediately to any change in capacitance which
is correlated to total water or moisture content in oil.
For
product information, please refer to http://www.eesiflo.com/products/easz1_01.html
Or
call your nearest EESIFLO representative office